Appropriate solvent NaVO3 for composition analysis of LiNbO 3 crystal using chemical method

De Long Zhang; Jian Gao; Ping Rang Hua; Dao Yin Yu; Edwin Yue Bun Pun

doi:10.1021/ac303514f

Appropriate solvent NaVO₃ for composition analysis of LiNbO ₃ crystal using chemical method

De Long Zhang^*
, Jian Gao
, Ping Rang Hua
, Dao Yin Yu
, Edwin Yue Bun Pun

^*Corresponding author for this work

Tianjin University
City University of Hong Kong

Research output: Contribution to journal › Article › peer-review

3 Scopus citations

Abstract

It is crucial to find an appropriate solvent for composition analysis of LiNbO₃ crystal by a chemical method, such as inductively coupled plasma atomic emission spectroscopy. We have comparatively studied several solvents for LiNbO₃ crystal, including HF acid, KHSO₄, B₂O₃, LiBO₂, and NaVO₃. The results show that as the NaVO₃ is used as the solvent, the solubility of LiNbO₃ is as high as 1 g/g at 1000 C. The dissolving is quite fast. Neither solute nor solvent is lost from the melting during the dissolving procedure. A clear high-concentration solution is obtained. Moreover, it is verified experimentally that such a solution is valid for composition analysis of LiNbO₃ crystal by a chemical method. In contrast, the other solvents suffer from one problem or another. We conclude that NaVO₃ is an appropriate solvent for chemical analysis of LiNbO₃.

Original language	English
Pages (from-to)	1940-1944
Number of pages	5
Journal	Analytical Chemistry
Volume	85
Issue number	3
DOIs	https://doi.org/10.1021/ac303514f
State	Published - 5 Feb 2013
Externally published	Yes

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title = "Appropriate solvent NaVO3 for composition analysis of LiNbO 3 crystal using chemical method",

abstract = "It is crucial to find an appropriate solvent for composition analysis of LiNbO3 crystal by a chemical method, such as inductively coupled plasma atomic emission spectroscopy. We have comparatively studied several solvents for LiNbO3 crystal, including HF acid, KHSO4, B2O3, LiBO2, and NaVO3. The results show that as the NaVO3 is used as the solvent, the solubility of LiNbO3 is as high as 1 g/g at 1000 C. The dissolving is quite fast. Neither solute nor solvent is lost from the melting during the dissolving procedure. A clear high-concentration solution is obtained. Moreover, it is verified experimentally that such a solution is valid for composition analysis of LiNbO3 crystal by a chemical method. In contrast, the other solvents suffer from one problem or another. We conclude that NaVO3 is an appropriate solvent for chemical analysis of LiNbO3.",

author = "Zhang, \{De Long\} and Jian Gao and Hua, \{Ping Rang\} and Yu, \{Dao Yin\} and Pun, \{Edwin Yue Bun\}",

year = "2013",

month = feb,

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doi = "10.1021/ac303514f",

language = "英语",

volume = "85",

pages = "1940--1944",

journal = "Analytical Chemistry",

issn = "0003-2700",

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TY - JOUR

T1 - Appropriate solvent NaVO3 for composition analysis of LiNbO 3 crystal using chemical method

AU - Zhang, De Long

AU - Gao, Jian

AU - Hua, Ping Rang

AU - Yu, Dao Yin

AU - Pun, Edwin Yue Bun

PY - 2013/2/5

Y1 - 2013/2/5

N2 - It is crucial to find an appropriate solvent for composition analysis of LiNbO3 crystal by a chemical method, such as inductively coupled plasma atomic emission spectroscopy. We have comparatively studied several solvents for LiNbO3 crystal, including HF acid, KHSO4, B2O3, LiBO2, and NaVO3. The results show that as the NaVO3 is used as the solvent, the solubility of LiNbO3 is as high as 1 g/g at 1000 C. The dissolving is quite fast. Neither solute nor solvent is lost from the melting during the dissolving procedure. A clear high-concentration solution is obtained. Moreover, it is verified experimentally that such a solution is valid for composition analysis of LiNbO3 crystal by a chemical method. In contrast, the other solvents suffer from one problem or another. We conclude that NaVO3 is an appropriate solvent for chemical analysis of LiNbO3.

AB - It is crucial to find an appropriate solvent for composition analysis of LiNbO3 crystal by a chemical method, such as inductively coupled plasma atomic emission spectroscopy. We have comparatively studied several solvents for LiNbO3 crystal, including HF acid, KHSO4, B2O3, LiBO2, and NaVO3. The results show that as the NaVO3 is used as the solvent, the solubility of LiNbO3 is as high as 1 g/g at 1000 C. The dissolving is quite fast. Neither solute nor solvent is lost from the melting during the dissolving procedure. A clear high-concentration solution is obtained. Moreover, it is verified experimentally that such a solution is valid for composition analysis of LiNbO3 crystal by a chemical method. In contrast, the other solvents suffer from one problem or another. We conclude that NaVO3 is an appropriate solvent for chemical analysis of LiNbO3.

UR - https://www.scopus.com/pages/publications/84873325519

U2 - 10.1021/ac303514f

DO - 10.1021/ac303514f

M3 - 文章

AN - SCOPUS:84873325519

SN - 0003-2700

VL - 85

SP - 1940

EP - 1944

JO - Analytical Chemistry

JF - Analytical Chemistry

IS - 3

ER -

Appropriate solvent NaVO₃ for composition analysis of LiNbO ₃ crystal using chemical method

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